Antioxidant3114 CAS 27676-62-6

Introduction:Basic information about Antioxidant3114 CAS 27676-62-6, including its chemical name, molecular formula, synonyms, physicochemical properties, and safety information, etc.

Antioxidant3114 Basic informationFeatures

Product Name:Antioxidant3114
Synonyms:1,3,5-triazine-2,4,6(1h,3h,5h)-trione,1,3,5-tris[[3,5-bis(1,1-dimethylethyl)-4;3,5-Triazine-2,4,6(1H,3H,5H)-trione,1,3,5-tris[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]methyl]1;Antioxidant3114;-hydroxyphenyl]methyl]-;1,3,5-Tris(3,5-di-tert-butyl-4-hydroxybenzyl)isocyanuric acid;AgeRite GT;Mark AO-20;1,3,5-Tris(3',5'-di-t-butyl-4-hydroxybenzyl)isocyanuric acid
CAS:27676-62-6
MF:C48H69N3O6
MW:784.08
EINECS:248-597-9
Product Categories:Organics;Industrial/Fine Chemicals;Antioxidant
Mol File:27676-62-6.mol

Antioxidant3114 Chemical Properties

Melting point 218-220 °C(lit.)
Boiling point 757.9±60.0 °C(Predicted)
density 1.03g/cm3
vapor pressure 0Pa at 25℃
Fp 289°C
storage temp. Inert atmosphere,Room Temperature
solubility Chloroform (Slightly), Ethyl Acetate (Slightly, Heated), Methanol (Slightly, Heated)
pka11.45±0.40(Predicted)
form solid
color White to Off-White
Water Solubility 40μg/L at 20℃
Major Applicationpharmaceutical (small molecule)
InChIKeyVNQNXQYZMPJLQX-UHFFFAOYSA-N
SMILESN1(CC2=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C2)C(=O)N(CC2=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C2)C(=O)N(CC2=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C2)C1=O
LogP15.18
CAS DataBase Reference27676-62-6(CAS DataBase Reference)
EPA Substance Registry System1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3,5-tris[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]methyl]- (27676-62-6)

Safety Information

WGK Germany -
TSCA TSCA listed
HS Code 2933690000
Storage Class11 - Combustible Solids

Antioxidant3114 Usage And Synthesis

FeaturesAntioxidant 3114 is a hindered phenol antioxidant with light and heat stability, low volatility and anti-aging properties. It can produce synergistic effects when used in combination with UV absorbers and phosphites.
Chemical PropertiesWhite to Light yellow powder to crystal
UsesTris(3,5-di-tert-butyl-4-hydroxybenzyl) Isocyanurate(Antioxidant3114) is used an as antioxidant-stabilizer in polyolefin films intended for packaging nonfatty food as well as an antioxidant in propylene copolymers.
UsesTris(3,5-di-tert-butyl-4-hydroxybenzyl) Isocyanurate is used an as antioxidant-stabilizer in polyolefin films intended for packaging nonfatty food as well as an antioxidant in propylene copolymers.
General DescriptionAntioxidant 3114, chemically known as Tris(3,5-di-tert-butyl-4-hydroxybenzyl) isocyanurate, serves as an effective antioxidant and UV stabilizer. It is extensively utilized in various materials including polyethylene, polypropylene, polystyrene, ABS resin, polyester, nylon, polyurethane, rubber, adhesives, petroleum resins, coatings, and oils. Additionally, it functions as a free radical scavenger to enhance the stability of polyolefins.
Flammability and ExplosibilityNon flammable
Synthesis

50-00-0

108-80-5

128-39-2

27676-62-6

To a 1L autoclave equipped with a mechanical stirrer, a thermometer socket, a manometer and a nitrogen displacement port, 178 g of 2,6-di-tert-butylphenol, 24.48 g of paraformaldehyde, 41.28 g of isocyanuric acid, and 4.4 g of urotropine were added sequentially. The system was vacuumed and nitrogen replacement was repeated more than three times, and after the last nitrogen replacement, 1000 mL of 70% v/v methanol aqueous solution was pumped into the reactor under -0.01 MPa negative pressure. Subsequently, the system was charged with nitrogen to a pressure of 0.6 MPa. Under the nitrogen atmosphere, the temperature was gradually increased to 120°C and maintained for 2 hours, and then continued to increase to 140°C and maintained for 4 hours to complete the reaction. At the end of the reaction, the reactor was cooled to 58°C by circulating water to obtain the crude product. After the crude product was filtered, the solid was dissolved in 70% by volume methanol aqueous solution, cooled and recrystallized. The recrystallized product was washed at least twice with anhydrous methanol at 55 °C and dried to give the white crystalline target product, hindered phenolic antioxidant 3114, in 92.3% yield.

References[1] Patent: CN108707122, 2018, A. Location in patent: Paragraph 0020; 0021; 0028; 0029

Antioxidant3114 Preparation Products And Raw materials

Raw materialsParaformaldehyde-->Cyanuric acid-->2,6-Di-tert-butylphenol-->Formaldehyde-->Hexamethylenetetramine-->Methanol-->Water
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