Cyclohexylhydrazine hydrochloride CAS 24214-73-1
Introduction：Basic information about Cyclohexylhydrazine hydrochloride CAS 24214-73-1, including its chemical name, molecular formula, synonyms, physicochemical properties, and safety information, etc.
Cyclohexylhydrazine hydrochloride Basic information
| Product Name: | Cyclohexylhydrazine hydrochloride |
| Synonyms: | CYCLOHEXYLHYDRAZINE HYDROCHLORIDE;1-CYCLOHEXYLHYDRAZINE HYDROCHLORIDE;CyclohexylhydrazineHCl;Hydrazinocyclohexane hydrochloride;Hydrazine, cyclohexyl-,hydrochloride (1:1);Cyclohexylhydrazine hydrochloride 98%;Cyclohexylhydrazine hydrochloride≥ 98%(Titration);Cyclohexylhydrazine monohydrochloride |
| CAS: | 24214-73-1 |
| MF: | C6H15ClN2 |
| MW: | 150.65 |
| EINECS: | |
| Product Categories: | Hydrazines;Nitrogen Compounds;Organic Building Blocks |
| Mol File: | 24214-73-1.mol |
Cyclohexylhydrazine hydrochloride Chemical Properties
| Melting point | 110-114 °C(lit.) |
| storage temp. | under inert gas (nitrogen or Argon) at 2–8 °C |
| form | Crystalline Powder |
| color | White |
| Water Solubility | almost transparency |
| InChI | InChI=1S/C6H14N2.ClH/c7-8-6-4-2-1-3-5-6;/h6,8H,1-5,7H2;1H |
| InChIKey | JZRHODNPRNTXKO-UHFFFAOYSA-N |
| SMILES | C1(NN)CCCCC1.Cl |
| CAS DataBase Reference | 24214-73-1(CAS DataBase Reference) |
Safety Information
| Hazard Codes | C |
| Risk Statements | 34 |
| Safety Statements | 26-36/37/39-45 |
| RIDADR | UN 3263 8/PG 2 |
| WGK Germany | 3 |
| HazardClass | 8 |
| PackingGroup | Ⅱ |
| HS Code | 29280000 |
| Storage Class | 8A - Combustible corrosive hazardous materials |
| Hazard Classifications | Skin Corr. 1B |
| Chemical Properties | White to light yellow powder,crystals or |
| Synthesis | 60295-21-8 24214-73-1 GENERAL METHOD: tert-Butyl 2-cyclohexylhydrazine-1-carboxylate (1.9 g, 8.87 mmol) was dissolved in dioxane and to this solution was added a dioxane solution (20 mL) of 4 M HCl. The reaction mixture was heated to reflux and stirred overnight. Upon completion of the reaction, it was cooled to room temperature, the precipitated white precipitate was collected by filtration, washed with a small amount of cold dioxane and dried to give cyclohexylhydrazine hydrochloride (1.8 g, yield: >100%) as a white solid. |
| References | [1] Patent: WO2016/123392, 2016, A2. Location in patent: Paragraph 00476 [2] Patent: WO2014/82598, 2014, A1. Location in patent: Paragraph 0419 [3] Journal of Organic Chemistry, 1981, vol. 46, # 26, p. 5413 - 5414 [4] Patent: WO2005/40169, 2005, A2. Location in patent: Page/Page column 150 |
Cyclohexylhydrazine hydrochloride Preparation Products And Raw materials
| Raw materials | Hydrazinecarboxamide, 2-(5-hydroxycyclooctylidene)--->TERT-BUTYL 2-CYCLOHEXYLHYDRAZINECARBOXYLATE-->tert-butyl 2-cyclohexylidenehydrazinecarboxylate-->Hydrochloric acid-->1,4-Dioxane |
| Preparation Products | 5-aMino-1-cyclohexyl-1h-pyrazole-4-carboxaMide-->2-CYCLOHEXYL-5-METHYL-2H-PYRAZOL-3-YLAMINE |
