Phenylmethyl methanesulfonate CAS 55791-06-5
Introduction：Basic information about Phenylmethyl methanesulfonate CAS 55791-06-5, including its chemical name, molecular formula, synonyms, physicochemical properties, and safety information, etc.
Phenylmethyl methanesulfonate Basic information
| Product Name: | Phenylmethyl methanesulfonate |
| Synonyms: | Methanesulfonic acid, phenylmethyl ester;Phenylmethyl methanesulfonate;benzyl Methanesulfonate |
| CAS: | 55791-06-5 |
| MF: | C8H10O3S |
| MW: | 186.23 |
| EINECS: | |
| Product Categories: | |
| Mol File: | 55791-06-5.mol |
Phenylmethyl methanesulfonate Chemical Properties
| Boiling point | 98 °C(Press: 0.2 Torr) |
| density | 1.244±0.06 g/cm3(Predicted) |
| storage temp. | Store at room temperature |
| Appearance | Light yellow to light brown Oil |
Safety Information
| Synthesis | Phenylmethyl methanesulfonate was prepared by the reaction of Benzyl alcohol and Methanesulfonyl chloride[1]: 1.Dissolve (0.5 g, 4.6 mmol) of the benzyl alcohol in 20 ml of CH2Cl2 in a one neck round bottom flask and cool the mixture at 0 °C. 2.Add (1 eq, 4.6mmol) of triethylamine under stirring. 3.Add (1 eq, 4.6 mmol) of methane sulfonyl chloride dropwise under stirring. 4.Stir the mixture open flask for one hour and half at -15 °C. 5.Quench the reaction with 2 ml of HCl 1N and wash the solution with NaHCO3 saturated aqueous solution. 6.Extract the organic phase and wash three times with water. 7.Dry the organic phase over Na2SO4. 8.Remove the solvent under reduced pressure using a rotary evaporator. |
| References | [1] F. OLIVITO . Efficient synthesis of organic thioacetates in water1[J]. Organic & Biomolecular Chemistry, 2018, 16 41: Pages 7753-7759. DOI:10.1039/c8ob01896k. |
Phenylmethyl methanesulfonate Preparation Products And Raw materials
| Preparation Products | 4-BROMODIPHENYLMETHANE |
